4-氯乙酰乙酸乙酯文献综述和参考文献(2)

菜单

而2-氯乙酰乙酸乙酯的沸点和反应产品4-氯乙酰乙酸乙酯相差很少（在减压条件下约为2-3℃），因此在精馏纯化时通常要反复蒸馏，造成产品的大量分解，最终导致收率偏低。

参考文献

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