摘要：近年来随着发光材料的的发展以及各种先进荧光检测技术和仪器的应用,荧光材料已经开始成功地应用到高灵敏度的生物检测和生物成像等领域。针对这一情况,本论文采用水热法制备KY3F10纳米发光材料,对其发光性质进行了研究。 采用水热法在210℃下合成了 KY3F10纳米荧光粉,制备了不同浓度的 Sm3+,Tb3+稀土离子以及 Sm3+和 Tb3+共同掺杂的荧光粉。X 射线衍射（XRD），结果表明合成的样品均为纯KY3F10。光致发光（PL）光谱测试表明，成功合成了可以发绿光，红光和橙光的荧光粉。36041
毕业论文关键字： KY3F10；发光材料；水热法；光致发光
Preparation and properties of rare earth dopedfluoride powders
Abstract ：In recent years with luminescent materials development and application of variousadvanced fluorescence detection techniques and instruments, fluorescent material has begun tosuccessfully applied to high sensitivity of detection of biological and bio imaging field. In viewof this, hydrothermal synthesis of KY3F10 nanometer luminescent materials is used in thisthesis, and the luminescent properties of the luminescent materials are studied.. 16h nano -phosphors were synthesized by hydrothermal method at 210, KY3F10,, Sm3+, Tb3+ rare earthion and Sm3+, Tb3+, and the co - doped phosphors were prepared.. X ray diffraction (XRD)was used to analyze the samples, the results showed that the samples were pure KY3F10.Photoluminescence (PL) spectra of the tests show that, we successfully synthesized thefluorescent powder of green, red and orange
.Keyword: KY3F10；luminescence；hydrothermal method；photoluminescence
目录
第一章文献综述.1
1.1本论文的背景1
1.1.1荧光粉的分类.2
1.1.2荧光粉的应用.5
1.1.3荧光粉的研究现状5
1.2主要实验方法和研究进展10
1.2.1水热法10
1.2.2KY3F10国内外研究现状.12
1.3选题依据及主要工作19
1.3.1选题依据.19
1.3.2拟开展的研究内容19
第二章KY3F10纳米颗粒的制备及发光特性20
2.1实验部分20
2.1.1实验试剂及仪器设备.20
2.1.2实验步骤及流程.21
2.3结果和讨论23
2.3.1XRD图谱及分析23
2.3.2掺杂Sm3+稀土离子光谱图及分析.24
2.3.3掺杂Tb3+稀土离子光谱图及分析25
2.3.4以Tb3+为变量的Tb3+和Sm3+共掺杂光谱图及分析27
2.3.5以Sm3+为变量的Tb3+和Sm3+共掺杂光谱图及分析.28
2.3.6样品的色坐标图表.29
第三章结论和展望.30
3.1结论30
3.2展望30
致谢.31
参考文献.32 稀土掺杂氟化物粉体制备及性能研究:http://www.751com.cn/cailiao/lunwen_34344.html