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摘要本文采用电泳沉积法制备纳米Al/CuO复合薄膜，并对其电泳沉积条件及影响因素进行研究。制作了两种阴极电极，分别为喷墨打印技术制备的银基底玻片和图形反转工艺制备的铂基底玻片。
本次实验，首先，利用导电银线作为阴极测试电泳沉积的可行性及沉积条件，并对其影响因素进行研究。其次，将铂电极作为阴极进行电泳沉积纳米Al/CuO，利用X射线衍射（XRD）和激光共聚显微镜（CLSM）对纳米Al/CuO含能薄膜进行了表征。然后，使用高速摄影仪对纳米Al/CuO薄膜燃烧进行了初步研究和观察。最后，尝试制备特定形状与厚度的纳米Al/CuO含能薄膜用于研究其在微尺度下的燃烧及分解反应特性。68284
通过电泳沉积实验，验证了电泳沉积的可行性，并且确定了后续实验中沿用的实验条件。
毕业论文关键词：电泳沉积，纳米Al/CuO复合薄膜，薄膜表征。
毕业设计说明书（论文）外文摘要
Title Electrophoretic Deposition of Al / CuO composites
Abstract
This article prepared Al/CuO composites with electrophoretic deposition, and studied its deposition parameterss. Two kinds of cathode electrodes are prepared, respectively, for the silver inkjet printing substrate slides and graphics inversion process for preparing platinum substrate slide preparation techniques.
Firstly, the conductive silver wires were used as the cathode to test the feasibility of electrophoretic deposition and the deposition conditions, as well as its impact factors. Secondly, the platinum electrode is used as a cathode for the electrophoretic deposition of Al/CuO. Then, Al/CuO energetic films were characterized by X-ray diffraction (XRD) and confocal laser scanning microscopy (CLSM). Afterwards, using the high speed camera to research the burning phenomenon of Al/CuO films preliminarily. Lastly, by attempting to prepare a particular shape or thickness of Al/CuO energetic films, they are used to study the combustion and decomposition reaction characteristics under micro scales.
By electrophoretic deposition experiment, the feasibility of electrophoretic deposition is accepted, and the experimental conditions adopted in subsequent experiments are determined, too.
Key word: electrophoretic deposition, Al/CuO composite films, characterization
目录
1 绪论 1
1.1纳米铝热剂国内外研究情况 1
1.2 电泳沉积技术研究现状 2
1.3本文主要研究内容 2
2 纳米Al/CuO复合薄膜的制备 3
2.1纳米Al/CuO薄膜制备原理 3
2.2 阴极基底制备工艺 6
2.2.1 银基底制备工艺 6
2.2.2铂基底制备工艺 8
2.3实验装置与材料 14
2.3.1纳米Al/CuO薄膜制备装置 14
2.3.2燃烧试验装置 15
2.3.3药品参数 16
2.4薄膜制备相关数据计算 16
2.5 纳米Al/CuO薄膜制备工艺流程 17
3电泳沉积制备纳米Al/CuO薄膜条件的测试 19
3.1超声时间研究 19
3.2电压测试